Reaction Attempts Book
List of all experiments
NOTE: All solubility experiments by the Bradley group past this point are recorded on the ONS challenge wiki
Exp257 Synthesis of UC176C in ethyl acetate - KhalidExp256 Synthesis of UC176C in benzene - Khalid
Exp255 Synthesis of UC176C in methanol and benzene - Khalid
Exp254 Kinetic study for the formation UC176C in methanol via a Ugi reaction - Khalid
Exp253 Synthesis of three Ugi products UC176C in methanol - Khalid
Exp252 Kinetic study of Ugi reaction for the formation of UC176C in benzene - Khalid
Exp251 Synthesis of three Ugi products , UC176C, 148C and 150D - Khalid
Exp250 Synthesis of a Ugi product in benzene - Khalid
Exp249 Kinetic study of Ugi reaction in benzene - Khalid
Exp248 Synthesis of methyl ester of L-tryptophan- Khalid
Exp247 Synthesis of 10 Ugi products in THF - Khalid
Exp246 Kinetic study of Ugi reaction in benzene - Khalid
Exp245 Synthesis of top 20 Ugi products in methanol - Khalid
Exp244 Synthesis of 2 Ugi products in benzene - Marshall Moritz
Exp243 Oxidation of 1-phenylethanol with NaH -Khalid, Marshall
Exp242 Synthesis of 10 Ugi products in benzene with phenanthrene-9-carboxaldehyde - Marshall Moritz
Exp241 Ugi synthesis of 38 Ugi products in methanol - Khalid
Exp240 Ugi synthesis of 12 Ugi products in THF with phenanthrene-9-carboxaldehyde - Khalid
Exp239 Synthesis of a Ugi product in benzene with phenanthrene-9-carboxaldehyde - Marshall Moritz
Exp238 Ugi synthesis of 44 Ugi products in THF with phenanthrene-9-carboxaldehyde as aldehyde component - Khalid, Cedric
Exp237 Ugi synthesis of a Ugi product in methanol and THF with phenanthrene-9-carboxaldehyde - Khalid
Exp236 Ugi synthesis of 28 Ugi products in methanol - Khalid
Exp235 Ugi synthesis of two Ugi products in methanol - Khalid, Jenna
Exp234 Ugi synthesis of ten Ugi products in methanol (Ugi Reaction Blog#002) - David
Exp233 Ugi synthesis of six Ugi products in methanol (Ugi Reaction Blog#001) - David
Exp232 Ugi synthesis of 75 Ugi products in methanol - Khalid
Exp231 Ugi synthesis of nine Ugi products from the top 20 list of Sortase inhibitors - Khalid
Exp230 Ugi synthesis of four Ugi products in eight solvents at three concentrations - David
Exp229 Ugi synthesis of two new Ugi products in methanol - David
Exp228 Ugi synthesis of seven Ugi products six of them were in the top 20 list of Sortase inhibitors - Khalid
Exp227 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid - Khalid
Exp226 Ugi synthesis of eight Ugi products with1-pyrenebutyric acid - David
Exp225 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid- Khalid
Exp224 Ugi synthesis of eight Ugi products with 1-pyrenebutyric acid- Khalid
Exp223 Ugi synthesis of previously made 62E - David
Exp222 Effect of solvent and conc on few Ugi reactions- Khalid
Exp221 Effect of solvent and conc on few Ugi reactions - Khalid
Exp220 Effect of solvent and conc on few Ugi reactions - Khalid
Exp219 Three Ugi reactions involving 4-pyrenebutanoic acid in a bisolvent system (methanol/THF) - Khalid
Exp218 To test if deuterated methanol, acetone, chloroform and benzene can be distinguished by smell - Khalid
Exp217 Effect of THF as solvent on for 4 Ugi reaction, Effect of DMSO as a solvent on a Ugi reaction. - Khalid
Exp216 Ugi synthesis of ten previously made and three new Ugi products. - Khalid
Exp215 Ugi synthesis of nine Ugi products. - Khalid
Exp214 Ugi synthesis of previously made 150D using phenanthrene-9-carboxaldehyde, crotonic acid, benzylamine and t-butylisocyanide - Khalid
Exp213 Solubility of 4-chlorobenzaldehyde in chloroform and methanol by UV spectroscopy - Khalid
EXP212 Solubility measurements of p-nitrobenzaldehyde in different solvents. Tim
EXP211 Solubility estimation by UV-VIS Khalid
EXP210 Solubility estimation in methanol and ethanol Khalid
EXP209 Determination of the time parameter for chloroform containing solutions in speedvac. Khalid/Tim
EXP208 Solubility measurements of 9 aldehydes in 6 different solvents. Khalid/Tim
EXP207 Solubility measurements of boc-gly, vanillin and other compounds in methanol, ethanol and THF JCB
Exp206 Purification of the ugi product - Khalid
Exp205 Solubilities of 10 aldehydes in methanol -Tim and Khalid
Exp204 Determination of solubility of Ugi adduct (99C) in Methanol, Ethanol, Acetonitrile, Tetrahydrofuran, Acetone, Hexane, Chloroform, and Distilled Water - Cedric and Aneta
Exp203 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp202 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp201 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp200 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide (verified by TomO) - Khalid
Exp199 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide (verified by TomO) - Khalid
Exp198 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp197 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp196 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp195 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp194 missing
Exp193 missing
Exp192 Optimization of a Ugi reaction involving Benzaldehyde, Furfurylamine, Boc-Glycine and tert-butyl isocyanide - Khalid
Exp191 Repeat of Exp189 - Khalid
Exp190 42 Ugi reactions on Minimapper -Trial 2 - Khalid
Exp189 Ugi reaction optimization using MiniMapper - Trial 1 - Khalid
Exp188 Ugi synthesis- Effect of Concentration - Khalid
Exp187Ugi synthesis- Effect of Concentration - Khalid
Exp186 Ugi synthesis (V2 Rank 83) using benzaldehyde, aniline, 1-pyrenebutyric acid and n-butylisocyanide-Emily
Exp185 Ugi synthesis- Effect of Concentration - Khalid
Exp184 Ugi synthesis (V1 Rank 49) using phenanthrene-9-carboxaldehyde, cyclohexylamine, mandelic acid and t-butyl isocyanide- Emily
Exp183 Ugi synthesis (V1 Rank 49) using phenanthrene-9-carboxaldehyde, cyclohexylamine, mandelic acid and t-butyl isocyanide- Emily
Exp182 Ugi synthesis (V1 Rank 28) using heptylamine, phenanthrene-9-carboxaldehyde, furoic acid and n-butyl isocyanide- Emily
Exp181 Synthesis of compounds ranked 55-124 from library DEXP014-V2B Khalid
Exp180 Ugi synthesis (V1 Rank 40) using heptylamine, phenanthrene-9-carboxaldehyde, acetic acid and n-butyl isocyanide- Shannon
Exp179 Ugi synthesis (V1 Rank 44) using aniline, phenanthrene-9-carboxaldehyde, 4-chlorophenyl acetic acid and t-butyl isocyanide- Shannon
Exp178 Ugi synthesis (V1 Rank 29) using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Shannon
Exp177 Ugi synthesis (V1 Rank 38) using propylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Shannon
Exp176 !! Ugi synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Emily (ppt)
Exp175 Ugi synthesis using phenanthrene-9-carboxaldehyde, benzylamine, 4-chlorophenyl acetic acid and n-butyl isocyanide- Emily
Exp174 Synthesis of compounds ranked 31-54 (except 32,37) from library DEXP014-V2B Khalid
Exp173 Synthesis of compounds ranked 13-29 (except 23) from library DEXP014-V2B Khalid
Exp172 (aborted) Ugi synthesis using methyamine, B-methoxy-alpha-napthaldehyde, formic acid, and tosylmethyl isocyanide.-Lauren/Tim (repeat of Exp168)
Exp171 Synthesis of compounds ranked 1-12 from library DEXP014-V2B Khalid
Exp170 !! Ugi synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Emily
Exp169 !! Ugi synthesis using phenanthrene-9-carboxaldehyde, 3,4-methylenedioxyphenyl acetic acid, cyclohexylamine, and t-butyl isocyanide.-Tim
Exp168 !! Ugi synthesis using methyamine, B-methoxy-alpha-napthaldehyde, formic acid, and tosylmethyl isocyanide.-Tim
Exp167-!! Ugi synthesis using propylamine, phenanthrene-9-carboxaldehyde, 3,4-methylenedioxyphenyl acetic acid and n-butyl isocyanide- Tim.
Exp166 !! Plasmodium falciparum inhibition results for 2 Ugi products Jiri
Exp165 !! Falcipain-2 inhibition results for 2 Ugi products Jiri
Exp164 Ugi synthesis using aniline, phenanthrene-9-carboxaldehyde, phenyl acetic acid and n-butyl isocyanide- Emily/Shannon
Exp163 !! synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, mandelic acid, and tert-butyl isocyanide- Tim (repeat of Exp161)
Exp162 Ugi synthesis using phenanthrene-9-carboxaldehyde, cyclohexylamine, phenylacetic acid and t-butyl isocyanide (Repeat of Exp157)- Shannon
Exp161-!! synthesis using furfurylamine, phenanthrene-9-carboxaldehyde, mandelic acid, and tert-butyl isocyanide- Tim
Exp160 !! synthesis using phenanthrene-9-carboxaldehyde, furfurylamine, 3,4-dihydroxyphenyl acetic acid and n-butyl isocyanide- Emily
Exp159 Ugi synthesis using phenanthrene-9-carboxaldehyde, benzylamine, 4-chlorophenyl acetic acid and n-butyl isocyanide- Emily
Exp158 Ugi synthesis using 4-chlorobenzaldehyde, 5-methylfurfurylamine, salicylic acid and tosylmethyl isocyanide- Emily
Exp157 Ugi synthesis using phenanthrene-9-carboxaldehyde, cyclohexylamine, phenylacetic acid and t-butyl isocyanide- Shannon
Exp156 Ugi synthesis using phenanthrene-9-carboxaldehyde, crotonic acid, benzylamine and t-butyl isocyanide- Emily
Exp155 Ugi synthesis using benzaldehyde, 5-methyl-2-furylmethylamine, 3-(4-methoxyphenyl) propanioc acid, and t-butyl isocyanide- Tim/Emily
Exp154 Three attempts of Ugi synthesis- Shannon
Exp153 One attempt of Ugi synthesis -Mitesh
Exp151 One attempt of Ugi synthesis- Mitesh
Exp150 Ugi synthesis with Benzylamine, Phenanthrene-9-carboxaldehyde, Crotonic acid and tert-butyl isocyanide- Emily / Khalid
Exp149 ugi synthesis using phenanthrene -9- carboxaldehyde, hexylamine, benzoic acid and n-butylisocyanide., Aneh
Exp148 Ugi synthesis with Heptylamine, Phenanthrene-9-carboxaldehyde, Crotonic acid and tert-butyl isonitrile - Emily / Khalid
Exp147 Four attempts of Ugi synthesis - Mitesh/Rikesh
Exp146 Two attempts of Ugi synthesis - Rikesh/Mitesh
Exp144 Three attempts of Ugi synthesis - Rikesh/Mitesh
Exp143 Five attempts of Ugi synthesis - Emily
Exp142 Two attempts of Ugi synthesis - Rikesh/Mitesh
Exp141 Two attempts of Ugi synthesis - Rikesh/Mitesh
Exp140 Two attempts of Ugi synthesis - Emily
Exp139 Ten attempts of Ugi synthesis-aneh
Exp138 Three attempts of Ugi synthesis - Shannon
Exp137 Eight attempts of Ugi synthesis - Anett, Rikesh, Mitesh, Khalid
Exp136 Ugi synthesis using o-vanillin, benzylamine, Boc-Trp-OH, and n-pentylisocyanide - Mitesh/Rikesh
Exp135 Ugi synthesis using o-vanillin, hexylamine, Boc-Trp-OH, and benzyl isocyanide - Rikesh
Exp134 Four attempts of Ugi synthesis - Rikesh
Exp133 Synthesis of N-benzyl-N-(2-furylmethyl)acetamide - Khalid
Exp132 Synthesis of N-benzyl-N-[(5-methyl-2-furyl)methyl]acetamide - Khalid
Exp131 Nine Attempts of Ugi synthesis - Rikesh
Exp130 Five Attempts of Ugi synthesis - Rikesh
Exp129 Test for the stability of the furan ring of the acetamide of 5-methylfurfurylamine in TFA - Jessica
Exp128 Test for the stability of the furan ring of the acetamide of 5-methylfurfurylamine in TFA - Jessica
Exp127 Test for the stability of the furan ring of 109C Ugi adduct in TFA - Jessica
Exp126 Five attempts of Ugi synthesis - Jessica
Exp125 Three attempts of Ugi synthesis - Jessica
Exp124 Two attempts of Ugi synthesis - Khalid
Exp123 Ugi synthesis using furfuylamine, o-vanillin, Boc-Tryptophan, and n-butyl isocyanide - Jessica
Exp122 Ugi synthesis using methylamine, o-tolualdehyde, acetic acid, and p-toluenesulfonylmethyl isocyanide - Jessica
Exp121 Ugi synthesis using o-Vanillin, 5-methyl furfurylamine Boc-tryptophan and 1-pentylisocyanide- Khalid
Exp120 Ugi synthesis using o-Vanillin, furfurylamine Boc-tryptophan and 1-pentylisocyanide- Khalid
Exp119 Two attempts of Ugi synthesis - Jessica
Exp118 Purify propionaldehyde by distillation - Khalid
Exp117 Monitor Ugi synthesis using propionaldehyde, methylamine, acetic acid and tert-butyl isocyanide by NMR - Khalid
Exp116 Four attempts of Ugi synthesis - Khalid
Exp115 Monitor Ugi synthesis using furfural, methylamine, benzylisocyanide and α,4-dimethylphenylacetic acid by NMR - Khalid
Exp114 Ugi synthesis using furfuraldehyde, methylamine, benzylisocyanide and α,4-dimethylphenylacetic acid - Khalid
Exp113 Ugi synthesis using Benzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide, and Boc-glycine - Jessica
Exp112 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - Khalid / Jessica
Exp111 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - Khalid / Jessica
Exp110 Reaction of the Ugi product 108C with 50% TFA in CDCl3 (prolonged exposure) - Khalid / Jessica
Exp109 Ugi synthesis using 5-(Trifluoromethyl)-2-furylmethylamine, benzaldehyde, benzylisocyanide and boc-glycine - Khalid
Exp108 Ugi synthesis using furfurylamine, benzaldehyde, benzylisocyanide and boc-glycine - Khalid
Exp107 Tert-butylation of furfurylamine with t-butanol and Amberlyst 15(H) in CDCl3 at room temperature - Khalid
Exp106 Ugi synthesis using 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide and Boc-Gly-OH - Sean
Exp105 FriedelCrafts tert-butylation of N-(2-furylmethyl)acetamide-Khalid
Exp104 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp103 Synthesis of the acetamide of furfurylamine -Khalid
Exp102 FriedelCrafts tert-butylation of N-(2-furylmethyl)acetamide-Khalid
Exp101 Reaction of the Ugi product 99C with 50% TFA in CDCl3 (prolonged exposure) - Khalid
Exp100 Ugi synthesis using tert-butylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp099 Ugi synthesis using furfurylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp098 Reaction of the Ugi product 64C with 50% TFA in CDCl3 (prolonged exposure) - Khalid
Exp097 Reaction of the Ugi product 86B with 50% TFA in CDCl3 (prolonged exposure) - Khalid
Exp096 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp095 Ugi synthesis using furfurylamine, veratraldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp094 3,4-Dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Glycine, t-Butyl isocyanide (CHCl3 for imine, MeOH for rxn) - Sean
Exp093 Ugi synthesis using aniline, benzophenone, tert-butylisocyanide and boc-glycine - Khalid
Exp092 Test for the stability of the furan ring of amide of BocGlycine and 5MFA in 50% TFA - Khalid
Exp091 Reaction of the Ugi product 62E with 50% TFA in CDCl3. - Khalid
Exp090 Reaction of the Ugi product 62E with 10% TFA in CDCl3 - Alicia
Exp089 Ugi synthesis using tert-butylamine, benzaldehyde, tert-butylisocyanide and boc-glycine - Khalid
Exp088 Synthesis of an amide of Boc Glycine and 5-methylfurfurylamine in methanol-d4- Khalid
*Exp087 Synthesis of the Boc-deprotected amine of the Ugi product 86C- Khalid
Exp086 Benzaldehyde, 5-methylfurfurylamine, tert-butylisocyanide, Boc-glycine - Khalid
Exp085Crotonaldehyde, Methylfurfurylamine in CDCl3 - jgiammarco
Exp084Piperonal, Aniline, Boc-Gly-OH, Tertbutyalisocyanide in CDCl3- jgiammarco
Exp083Crotonaldehyde, Tertbutyalamine, Boc-Gly-OH, Tertbutylisocyanide in CDCl3- jgiammarco
Exp082 Synthesis of the Boc-deprotected amine of the Ugi product(64C-2) - Khalid
Exp081 Test for the stability of the furan ring of N-[(5-methyl-2-furyl)methyl]acetamide in 10% TFA - Khalid
Exp080 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutylisocyanide (CDCl3) -jgiammarco
Exp079 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - Alicia
Exp078 Synthesis of the acetamide of 5-methyl furfurylamine -Khalid
Exp077 Piperonal, tertbutylamine, Boc-Gly-OH(CDCl3) -jgiammarco
Exp076 Piperonal, tertbutylamine, Boc-Gly-OH (MeOH) -jgiammarco
Exp075 Perform a MALDI MS analysis of the Ugi product 62E - kgowens
Exp074 Synthesis of N-Cylohexenylformamide from Cylohexanone and formamide - Khalid
Exp073 Test for the stability of the furan ring of 5-Methylfurfurylamine in TFA - Khalid
Exp072 Ugi Product (diamide) Cycliztion using 10% HCl in CDCl3 - Alicia
Exp071 Synthesis of N-Cylohexenylformamide from Cylohexanone and formamide - Khalid
Exp070 Ugi Product (diamide) Cycliztion using 50% TFA in CDCl3 - Khalid
Exp069 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - jgiammarco
Exp068 Reaction of Boc-Glycine with 10%TFA in CDCl3 - Khalid
Exp067 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - Khalid
Exp066 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - jgiammarco
*Exp065 Ugi Product (diamide) Cycliztion using 10% TFA in CDCl3 - Alicia
*Exp064 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide, Boc-Gly-OH in MeOH - Khalid
*Exp063 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Gly-OH, benzyl isocyanide - Sean
*Exp062 Piperonal, 5-methylfurfurylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH - Alicia
*Exp061 3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, Boc-Gly-OH, t-butyl isocyanide - Sean
*Exp060 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide, Boc-Gly-OH in MeOH- Khalid
*Exp059 Piperonal, 5-methylfurfurylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH - Alicia
Exp058 Piperonal, tertbutylamine, Boc-Gly-OH, tertbutyl isocyanide in MeOH-d4 - jgiammarco
Exp057 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine in MeOH-d4) - Sean
Exp056 Boc-Met-OH and 5-Methyl furfurylamine in MeOH-d4 - Khalid
Exp055 Boc-Gly-OH and 5-Methyl furfurylamine in MeOH-d4 - Khalid
Exp054 [Veratraldehyde, 5-Methyl furfurylamine], Benzyl Isocyanide and final addition of Boc-Gly-OH in MeOH-d4 - Khalid
Exp053 Boc-Gly-OH and tert-butyl isocyanide in MeOH-d4 - Khalid
*Exp052 Piperonal, 5-methylfurfurylamine, BocGly-OH, tert-butyl isocyanide in MeOH - Alicia
Exp051 Piperonal and tert-butylamine, Boc-Gly-OH and dehydration with MgSO4 in MeOH-d4 - jgiammarco
Exp050 Boc-Gly-OH and Benzyl isocyanide in MeOH-d4 - Khalid
Exp049 Boc-Gly-OH and 2-morpholinoethyl isocyanide in MeOH-d4 - Khalid
Exp048 (piperonal, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in MeOH-d4) - jgiammarco
Exp047 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine in MeOH-d4) - Sean
Exp046 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in MeOH-d4) - Khalid
*Exp045 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3) - Khalid
Exp044 Formation of the imine of Phenyl acetaldehyde and tert-butylamine in CDCl3- Khalid
Exp043 Formation of the imine of Piperonal and 5-Methyl furfurylamine in MeOH-d4 - Alicia
Exp042 Formation of the imine of Phenyl acetaldehyde and tert-butylamine in CDCl3- Khalid / Lin
Exp041 Formation of the imine of Piperonal and 5-Methyl furfurylamine in MeOH-d4- Alicia
Exp040 Formation of the imine of Piperonal and 5-Methyl furfurylamine in CDCl3- Alicia
Exp039 Distillation of Phenylacetaldehyde (39B pure) - Khalid / Lin
Exp038 (Phenylacetaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3 ) - Alicia
Exp037 Distillation of Phenylacetaldehyde (contaminated)- jgiammarco
Exp036 Preparation of N-tert-butylphenylacetaldimine (impure by HMR)- Khalid
Exp035 Distillation of Phenylacetaldehyde(impure by HMR) - Khalid
Exp034 (Phenylacetaldehyde, 5-methylfurfurylamine, BocGly, 2-morpholinoethylisocyanide in CDCl3) - Alicia
Exp033 Distillation of Butyraldehyde (impure by HMR) - Alicia
Exp032 (Imine mix from Exp036, Boc-Met-OH, 2-morpholinoethylisocyanide in MeOH ) - Khalid
Exp031 (Phenylacetaldehyde after distillation, -methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) - jgiammarco
Exp030 (Piperonal, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in MeOH) - Khalid
Exp029 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH then CDCl3) - Alicia
Exp028 (Formaldehyde, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in 1M LiCl/Water) - Khalid
Exp027 (Formaldehyde, tertbutylamine, Boc-Gly-OH, 2-morpholino ethylisocyanide in Methanol) - Khalid
Exp026 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) Lin
EXP025 Convert adrenaline to DOPAL by acid catalysis - (2006-08-31) Khalid/Lin (pure without chromatography)
EXP024 Convert adrenaline to DOPAL by acid catalysis - Khalid/Lin
EXP023 (DOPAL, 5-methylfurfurylamine, N-(tert)-butoxycarbonyl)-L-methionine, and benzylisocyanide) - Khalid (crude)
EXP022 (3,4-dimethoxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) Khalid
EXP021 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) jgiammarco
EXP020 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH ) jgiammarco
EXP019 (Piperonal, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH) - Lin
EXP018 (3,4-dihydroxybenzaldehyde, 5-methylfurfurylamine, BocGly-OH, benzylisocyanide in MeOH) jgiammarco
EXP017 (Piperonal, 5-methylfurfurylamine, BocMet-OH, benzylisocyanide in MeOH) - Lin
EXP016 Convert adrenaline to DOPAL using phosphoric acid - jgiammarco
EXP015 Convert adrenaline to DOPAL using phosphoric acid - jgiammarco
EXP014 (Phenylacetaldehyde, 5-methylfurfurylamine, BocMet-OH, benzylisocyanide in MeOH) - Khalid
EXP013 Convert adrenaline to a catechol aldehyde using CH3COOH- jgiammarco
EXP012 Convert adrenaline to a catechol aldehyde using H2SO4- jgiammarco
EXP011 Convert adrenaline to a catechol aldehyde using H2SO4 and a benzene layer- jgiammarco
EXP010 Convert adrenaline to a catechol aldehyde using H2SO4 - jgiammarco
EXP009 Convert adrenaline to a catechol aldehyde using H2SO4, benzene, and water - jgiammarco
EXP008 Convert adrenaline to a catechol aldehyde using H2SO4 and benzene - jgiammarco
EXP007 Convert adrenaline to a catechol aldehyde using CH3COOH and H2SO4 - Alicia
EXP006 (Phenylacetaldehyde, 5-methylfurfurylamine, Boc-Met-OH, benzylisocyanide in MeOH) - Khalid
EXP005 Synthesis of 3,4-dihydroxyphenylacetaldehyde from adrenaline -jgiammarco
EXP004 Convert adrenaline to a catechol aldehyde using CH3COOH, H2SO4, and water - Brett
EXP003 (Phehylacetaldehyde, 5-methylfurfurylamine, Boc-Met-OH, benzylisocyanide in MeOH) - Brett/Alicia/jgiammarco
EXP002 Convert adrenaline to a catechol aldehyde using CH3COOH and H2SO4 - jgiammarco
EXP001 Convert adrenaline to a catechol aldehyde using MeOH - Jean-Claude Bradley
Usefulchem Table of Chemicals