ONS Challenge

Reaction Attempts: Advanced Search


Compound:
Solvent:
Reaction Type:
Researcher:
 

Reactions 
Reaction ID UCExp261-1
 
ResearcherEvan Curtin
Reaction Typeimine synthesis
Solventdichloromethane
Limiting Reactant0.8 M
PrecipitateNo
CommentsStirred RT 24h; attempt to recrystallize by adding hexane; no precipitate
Referencehttp://usefulchem.wikispaces.com/Exp261
 
+    
aniline benzaldehyde benzalaniline    

Reaction ID UCExp261-2
 
ResearcherEvan Curtin
Reaction Typeimine synthesis
Solventmethanol
Limiting Reactant0.8 M
PrecipitateNo
Yield66.5 %
CommentsStirred RT 24h; rotary evaporated; recrystallized in ethanol
Referencehttp://usefulchem.wikispaces.com/Exp261
 
+    
aniline benzaldehyde benzalaniline    

Reaction ID UCExp263
 
ResearcherEvan Curtin
Reaction Typeimine synthesis
Solventethanol
Limiting Reactant4 M
PrecipitateYes
Yield56.2 %
Commentshigh concentration led to layers; cooling to 0C gave precipitate
Referencehttp://usefulchem.wikispaces.com/Exp263
 
+    
aniline benzaldehyde benzalaniline    

3 Reactions Found