ONS Challenge

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Reactions 
Reaction ID SPUGI_002
 
ResearcherSebastian Petrik
Reaction Typereduction
Solventmethanol
Limiting Reactant -  M
PrecipitateNo
Yield12 %
Commentssuspension treated with Pd/C and H2 at 450psi 5h then filtered; evaporated and chromatographed
Referencehttp://sebastianpetrik.wikispaces.com/SPUGI_002
Solvent SelectionOptimal Solvent Prediction
 
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5-nitro-1,10-phenanthroline hydrogen 5-amino-1,10-phenanthroline    

Reaction ID SPUGI_001
 
ResearcherSebastian Petrik
Reaction Typenitration
Solventsulfuric acid
Limiting Reactant0.7 M
PrecipitateYes
Yield58 %
Comments7 eq. nitric acid at 160C; 4h then add ice; basify then acidify and filter precipitate
Referencehttp://sebastianpetrik.wikispaces.com/SPUGI_001
Solvent SelectionOptimal Solvent Prediction
 
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1,10-phenanthroline nitric acid 5-nitro-1,10-phenanthroline    

2 Reactions Found