##TITLE= STANDARD 1H OBSERVE ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 6.1 Revision B, December 4, 1998 $$ Thu Dec 28 13:42:59 EST 2006 $$ svsj version 5.1, 97/1/14 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= vxr3d ##OWNER= ##SPECTROMETER/DATA SYSTEM= Varian UNITY INOVA-300 ##.OBSERVE FREQUENCY= 300.0112289 ##.OBSERVE NUCLEUS= ^1H $$solvent=CDCl3 ##.FIELD= 7.05 $$ Tesla ##.ACQUISITION TIME= 3.7440000 $$ seconds ##.AVERAGES= 16 $$ number of transients ##RESOLUTION= 0.244 $$ digital resolution in Hz ##.SPINNING RATE= 20 $$ Hz ##.PHASE 0= -64.5 $$ zero order phase correction (left edge) ##.PHASE 1= 0.001816 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 499.955 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 101 0 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 3.744 ##$bs= 16 ##$celem= 1 ##$console= ##$cp= ##$ct= 16 ##$d1= 0 $$ sec ##$d2= 0 $$ sec ##$date= ##$dfrq= 300.0112289 $$ Hz ##$dm= ##$dmf= 200 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 30 ##$dres= 1 ##$dseq= <> ##$exppath= ##$fb= 2000 ##$file= ##$filter= 54.0999984741 ##$fn1= 1024 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$lcpeak_= 0 ##$load= ##$lockfreq_= 46.0536521 $$ Hz ##$lockgain_= 48 ##$lockphase_= 105 ##$lockpower_= 42 ##$math= ##$method= ##$np= 29952 ##$nt= 16 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$parversion= 5.1 ##$pmode= ##$priority= 5 ##$probe_= <4nuc_30122> ##$proc1= ##$proc= ##$pslabel= ##$pw90= 19.9999866486 $$ usec ##$pw= 6.9999961853 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$saveglobal_= (0..14) ##$seqfil= ##$sfrq= 300.0112289 ##$sn= 0 ##$solvent= ##$spin= 20 ##$ss= 0 ##$sw= 4000 ##$tin= ##$tn=

##$tof= 0 $$ Hz ##$tpwr= 55 ##$vloc_= ##$vproto_= <> ##$vrack_= 1 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$vzone_= 1 ##$wbs= <> ##$werr= <> ##$wexp= <> ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= 194 ##$x2y2= -62 ##$x3= -66 ##$x4= 0 ##$xy= 94 ##$xz2= 0 ##$xz= -117 ##$y1= 7 ##$y3= -76 ##$y4= 0 ##$yz2= 0 ##$yz= 272 ##$z0_= 855 ##$z1= 0 ##$z1c= -616 ##$z2= 0 ##$z2c= -1396 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 0 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= 0 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 1 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= -57.2 ##$lp= -7.3 ##$rfl= 500.0 ##$rfp= 0.0 ##$refpos= 0.0 ##$reffrq= 300.0 ##$axis=

##$sp= -500.0 ##$wp= 4000.0 ##$cr= 1129.0 ##$delta= 58.6 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.244140625 ##XUNITS= HZ ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 0.244140625000 ##YFACTOR= 0.004943753 ##FIRSTX= 3999.755859375 ##LASTX= 0.000000000 ##MAXY= 161.991958 ##MINY= -0.153256 ##NPOINTS= 16384 ##FIRSTY= 0.000000 ##XYDATA= (X++(Y..Y)) 16383@%TJjLlKmKk%TKjTKoQkLlLljMklOnLk%kNnJT%kOmlNkmM%oQmKTmLPol%jKTk%J%TlMmK%T 16311@nQpKLlJjMJ%k%j%WLljJmPoKJlOmMoMmKTj%lOl%mLMmjKJjJjlLJMnKkMnLjklMjKkNpLTn 16236bKJjLjlNlMnoQMolkOj%Kj%KnkPpNJKmTNJlkKkNjmOoLnQnNmM%mJTLnjJ%J%TKljkM%MnlM 16164@%j%J%TKJnK%JkJkNljJklNjnQkKknMkLTlkM%m%JKlKTk%lLmM%Ll%k%NnJL%k%UjlPl%Vkl 16089ePlLjUNoJT%TLlJmMNnkLJlMjl%Jm%TLJjTJMpLnNkKLm%jLTm%jJlMKnKlQqOnKj%KTkTjQ 16017Fj0N%j%Jj%VLl%MjnjNlJTj%KkKJkjkK%K%TmK%mJKJ%TLnOjlj%JKTljkLmjM%LnJ%KnPjkjT 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143Dm%Tk%TJoRk%KkTlN%UJLljKlJMrMOqLKkjTLmLlLkjNljM%ljKJmNJjk%mJPj0OlJNjnKMkl%J 69aLnLT%l%KmjLKkMlkJUjMrQmKklNkJMmJlJTjJjMml%KLlJlPj1OKm%OmKj%lKJ%TlLTlo 0f $$ checkpoint ##END= ##TITLE= STANDARD 1H OBSERVE ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 6.1 Revision B, December 4, 1998 $$ Tue Dec 19 18:09:27 EST 2006 $$ svsj version 5.1, 97/1/14 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= vxr3d ##OWNER= ##SPECTROMETER/DATA SYSTEM= Varian UNITY INOVA-300 ##.OBSERVE FREQUENCY= 300.0112289 ##.OBSERVE NUCLEUS= ^1H $$solvent=CDCl3 ##.FIELD= 7.05 $$ Tesla ##.ACQUISITION TIME= 3.7440000 $$ seconds ##.AVERAGES= 16 $$ number of transients ##RESOLUTION= 0.244 $$ digital resolution in Hz ##.SPINNING RATE= 20 $$ Hz ##.PHASE 0= -75.7 $$ zero order phase correction (left edge) ##.PHASE 1= 0.006073 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 499.955 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 101 6 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 3.744 ##$bs= 16 ##$celem= 1 ##$console= ##$cp= ##$ct= 16 ##$d1= 0 $$ sec ##$d2= 0 $$ sec ##$date= ##$dfrq= 300.0112289 $$ Hz ##$dm= ##$dmf= 200 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 30 ##$dres= 1 ##$dseq= <> ##$exppath= ##$fb= 2000 ##$file= ##$filter= 54.0999984741 ##$fn1= 1024 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$lcpeak_= 0 ##$load= ##$lockfreq_= 46.0536521 $$ Hz ##$lockgain_= 48 ##$lockphase_= 97 ##$lockpower_= 44 ##$math= ##$method= ##$np= 29952 ##$nt= 16 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$parversion= 5.1 ##$pmode= ##$priority= 5 ##$probe_= <4nuc_30122> ##$proc1= ##$proc= ##$pslabel= ##$pw90= 19.9999866486 $$ usec ##$pw= 6.9999961853 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$saveglobal_= (0..14) ##$seqfil= ##$sfrq= 300.0112289 ##$sn= 0 ##$solvent= ##$spin= 20 ##$ss= 0 ##$sw= 4000 ##$tin= ##$tn=

##$tof= 0 $$ Hz ##$tpwr= 55 ##$vloc_= ##$vproto_= <> ##$vrack_= 1 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$vzone_= 1 ##$wbs= <> ##$werr= <> ##$wexp= ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= 194 ##$x2y2= -62 ##$x3= -66 ##$x4= 0 ##$xy= 94 ##$xz2= 0 ##$xz= -117 ##$y1= 7 ##$y3= -76 ##$y4= 0 ##$yz2= 0 ##$yz= 272 ##$z0_= 845 ##$z1= -688 ##$z1c= -616 ##$z2= 1309 ##$z2c= -1504 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 170 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= -82 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 1 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= -51.4 ##$lp= -24.3 ##$rfl= 500.0 ##$rfp= 0.0 ##$refpos= 0.0 ##$reffrq= 300.0 ##$axis=

##$sp= -500.0 ##$wp= 4000.0 ##$cr= -0.6 ##$delta= 42.0 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.244140625 ##XUNITS= HZ ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 0.244140625000 ##YFACTOR= 0.004943995 ##FIRSTX= 3999.755859375 ##LASTX= 0.000000000 ##MAXY= 161.994945 ##MINY= -0.079104 ##NPOINTS= 16384 ##FIRSTY= 0.000000 ##XYDATA= (X++(Y..Y)) 16383@%s%TJj%s%s%TJj%UjJjJ%s%XjJ%s%s%s%s%s%s%s%s%s%s%VJj%XJj%s%s%WjJ%s%s%s%s%s 16150@%VjJ%s%YjJ%s%WjJ%s%s%s%YjJ%UjKj%s%UjJ%s%s%sjJ%s%YJj%UJj%YJj%UJj%s%UJj%TJ 15971A%Tj%VJjJj%J%UjJj%J%TjJTj%jJ%WjJ%JkJ%J%Uj%KkJTj%Jj%Jj%J%ZJ%sJ%j%JTj%TJ%jJ 15879FjJkK%TJT%jTJT%TjJT%TjJ%J%TJ%TjJ%UJ%Kj%TJT%j%JKjJ%TJT%TJT%J%TJTjJU%J%TJ%T 15805B8KjJ%J%J%JT%JT%JWK%KJUKJKJTLJTKLJTKJKTJKT%MjLKUJKTLKLKLVMTLMOLONONPNQPTR 15727B07J0PJ0TJ2TJ3J2J5TJ6J8J6K1UK3K7K6K8L1L2L4L5L9L8M3UM6UM7M6TM3M1TL5L2K6K3 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checkpoint ##END= ##TITLE= STANDARD 1H OBSERVE ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 6.1 Revision B, December 4, 1998 $$ Mon Dec 18 17:57:09 EST 2006 $$ svsj version 5.1, 97/1/14 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= vxr3d ##OWNER= ##SPECTROMETER/DATA SYSTEM= Varian UNITY INOVA-300 ##.OBSERVE FREQUENCY= 300.0112289 ##.OBSERVE NUCLEUS= ^1H $$solvent=CDCl3 ##.FIELD= 7.05 $$ Tesla ##.ACQUISITION TIME= 3.7440000 $$ seconds ##.AVERAGES= 16 $$ number of transients ##RESOLUTION= 0.244 $$ digital resolution in Hz ##.SPINNING RATE= 20 $$ Hz ##.PHASE 0= -83.8 $$ zero order phase correction (left edge) ##.PHASE 1= 0.003038 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 489.258 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 101 6 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 3.744 ##$bs= 16 ##$celem= 1 ##$console= ##$cp= ##$ct= 16 ##$d1= 0 $$ sec ##$d2= 0 $$ sec ##$date= ##$dfrq= 300.0112289 $$ Hz ##$dm= ##$dmf= 200 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 30 ##$dres= 1 ##$dseq= <> ##$exppath= ##$fb= 2000 ##$file= ##$filter= 54.0999984741 ##$fn1= 1024 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$lcpeak_= 0 ##$load= ##$lockfreq_= 46.0536521 $$ Hz ##$lockgain_= 48 ##$lockphase_= 97 ##$lockpower_= 44 ##$math= ##$method= ##$np= 29952 ##$nt= 16 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$parversion= 5.1 ##$pmode= ##$priority= 5 ##$probe_= <4nuc_30122> ##$proc1= ##$proc= ##$pslabel= ##$pw90= 19.9999866486 $$ usec ##$pw= 6.9999961853 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$saveglobal_= (0..14) ##$seqfil= ##$sfrq= 300.0112289 ##$sn= 0 ##$solvent= ##$spin= 20 ##$ss= 0 ##$sw= 4000 ##$tin= ##$tn=

##$tof= 0 $$ Hz ##$tpwr= 55 ##$vloc_= ##$vproto_= <> ##$vrack_= 1 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$vzone_= 1 ##$wbs= <> ##$werr= <> ##$wexp= <> ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= 194 ##$x2y2= -62 ##$x3= -66 ##$x4= 0 ##$xy= 94 ##$xz2= 0 ##$xz= -117 ##$y1= 7 ##$y3= -76 ##$y4= 0 ##$yz2= 0 ##$yz= 272 ##$z0_= 851 ##$z1= -2047 ##$z1c= -616 ##$z2= 1152 ##$z2c= -1504 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 170 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= -82 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 1 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= -71.7 ##$lp= -12.2 ##$rfl= 489.3 ##$rfp= 0.0 ##$refpos= 0.0 ##$reffrq= 300.0 ##$axis=

##$sp= -489.3 ##$wp= 4000.0 ##$cr= 0.0 ##$delta= 84.0 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.244140625 ##XUNITS= HZ ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 0.244140625000 ##YFACTOR= 0.004943978 ##FIRSTX= 3999.755859375 ##LASTX= 0.000000000 ##MAXY= 161.999334 ##MINY= -0.212591 ##NPOINTS= 16384 ##FIRSTY= 0.000000 ##XYDATA= (X++(Y..Y)) 16383@JjTJ%TJjJkJ%J%jTJ%KlJjJ%jKjKkJj%jJ%jKj%jJTj%Kk%UjJ%kL%kKkJjJ%UKklMj%UJjT 16308aKkjKjKkKj%Tj%LmK%jJ%KlJ%Tj%J%Jj%VjLk%JjkK%Kk%WJjT%J%lMj%JkJ%Wj%J%VKk%TKk 16226@JkJkK%JlKJjJj%TkK%TlMj%JjJkKkJT%Tj%VjJTjJ%j%TjKjTJ%JkJ%TkK%UJjTJ%WkK%UKl 16147aJ%WJlK%TLm%JjTKJjJjTJTj%WJ%j%TjJT%j%TjJjJkJTKk%JjkK%TJjJkJ%LmJjJ%UkLjKkj 16068aJ%UkKJjTK%Tj%Tj%J%WjJ%TjJkKJ%Tj%WjMkjJj%JlLkJ%jJjJkJ%JTj%UkKTl%KkJTj%jJj 15988aJ%kKTkJj%VJj%KlJT%Tk%jKJj%VkKTj%lJTjJ%j%NlkJ%ZJjkK%UjJK%nKTjTJkKjJjJjJ%J 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374AjKk%j%TJ%Kk%jJ%s%UJj%Kk%JjTKjJjJjkK%TKk%UJj%J%j%j%TJ%UJkJ%TJjT%TJ%JkKjTJ%T 290@j%K%j%TKjlK%WkKJ%jTJTj%VKkJjkLJlJ%WjJ%UjJ%jKj%JkLkJjTJ%jJ%TjJjT%KkK%UjTKJT 206BkjKkJ%s%UKkTJKjTJjJ%jJKjlK%UJj%UlL%VLlj%JjKjTJKkTJKjTJTjKk%Jj%XLkj%TkLk%JT 116AjJj%lJKLk%j%TkLkJKkJkJkKjJ%TjJUkjJTj%j%J%Jk%Kj%Uj%TK%j%UkKTjT%jJjJ%Jj%jJTk 39aJ%TKkJ%jT%K%jTKjkJT%Kk%XkK%TJj% 0@ $$ checkpoint ##END= ##TITLE= STANDARD 1H OBSERVE ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 6.1 Revision B, December 4, 1998 $$ Mon Dec 18 17:28:05 EST 2006 $$ svsj version 5.1, 97/1/14 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= vxr3d ##OWNER= ##SPECTROMETER/DATA SYSTEM= Varian UNITY INOVA-300 ##.OBSERVE FREQUENCY= 300.0112289 ##.OBSERVE NUCLEUS= ^1H $$solvent=CDCl3 ##.FIELD= 7.05 $$ Tesla ##.ACQUISITION TIME= 3.7440000 $$ seconds ##.AVERAGES= 16 $$ number of transients ##RESOLUTION= 0.244 $$ digital resolution in Hz ##.SPINNING RATE= 20 $$ Hz ##.PHASE 0= -71.2 $$ zero order phase correction (left edge) ##.PHASE 1= 0.004193 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 467.285 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 101 6 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 3.744 ##$bs= 16 ##$celem= 1 ##$console= ##$cp= ##$ct= 16 ##$d1= 0 $$ sec ##$d2= 0 $$ sec ##$date= ##$dfrq= 300.0112289 $$ Hz ##$dm= ##$dmf= 200 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 30 ##$dres= 1 ##$dseq= <> ##$exppath= ##$fb= 2000 ##$file= ##$filter= 54.0999984741 ##$fn1= 1024 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$lcpeak_= 0 ##$load= ##$lockfreq_= 46.0536521 $$ Hz ##$lockgain_= 48 ##$lockphase_= 155 ##$lockpower_= 40 ##$math= ##$method= ##$np= 29952 ##$nt= 16 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$parversion= 5.1 ##$pmode= ##$priority= 5 ##$probe_= <4nuc_30122> ##$proc1= ##$proc= ##$pslabel= ##$pw90= 19.9999866486 $$ usec ##$pw= 6.9999961853 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$saveglobal_= (0..14) ##$seqfil= ##$sfrq= 300.0112289 ##$sn= 0 ##$solvent= ##$spin= 20 ##$ss= 0 ##$sw= 4000 ##$tin= ##$tn=

##$tof= 0 $$ Hz ##$tpwr= 55 ##$vloc_= ##$vproto_= <> ##$vrack_= 1 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$vzone_= 1 ##$wbs= <> ##$werr= <> ##$wexp= <> ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= 194 ##$x2y2= -62 ##$x3= -66 ##$x4= 0 ##$xy= 94 ##$xz2= 0 ##$xz= -117 ##$y1= 7 ##$y3= -76 ##$y4= 0 ##$yz2= 0 ##$yz= 272 ##$z0_= 841 ##$z1= -886 ##$z1c= -616 ##$z2= 352 ##$z2c= -1504 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 170 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= -82 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 1 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= -54.4 ##$lp= -16.8 ##$rfl= 467.3 ##$rfp= 0.0 ##$refpos= 0.0 ##$reffrq= 300.0 ##$axis=

##$sp= -467.3 ##$wp= 4000.0 ##$cr= 0.0 ##$delta= 162.9 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.244140625 ##XUNITS= HZ ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 0.244140625000 ##YFACTOR= 0.004614405 ##FIRSTX= 3999.755859375 ##LASTX= 0.000000000 ##MAXY= 151.200214 ##MINY= -0.032301 ##NPOINTS= 16384 ##FIRSTY= 0.000000 ##XYDATA= (X++(Y..Y)) 16383@%s%s%s%XJj%s%s%s%s%s%s%VJj%s%s%s%s%s%s%s%s%s%s%WJj%s%s%s%s%s%s%s%YjJ%s%s 16101@%s%s%s%s%s%s%s%s%TJj%s%s%s%s%s%s%s%s%WJj%s%s%s%s%TjJ%s%s%s%s%s%s%s%s%s%s 15816@%s%s%s%s%s%s%s%s%VjJ%sJj%s%s%jJ%s%ZJj%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s 15525@%s%s%s%s%s%Jj%s%TjJ%s%s%s%s%s%s%WJj%s%UjJ%s%XJj%s%s%s%s%s%s%s%s%s%s%s%s%s 15255@%s%s%Jj%sjT%J%J%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s 14958@%TJj%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%VJTjT%WjJ%sJjJj%s%s%s 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1136@%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s 803@%s%s%s%s%s%s%s%s%s%s%s%XjJ%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%Y 482@jJ%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%ZJj%s%s%s%s%TjJ%s%s%s%s%s%TjJ%W 196@jJ%XjJjJ%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s%s% 0@ $$ checkpoint ##END= ##TITLE= STANDARD 1H OBSERVE ##JCAMP-DX= 5.00 $$ Varian Associates, Inc., VNMR Software $$ VNMR Version 6.1 Revision B, December 4, 1998 $$ Tue Dec 19 18:31:30 EST 2006 $$ svsj version 5.1, 97/1/14 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= vxr3d ##OWNER= ##SPECTROMETER/DATA SYSTEM= Varian UNITY INOVA-300 ##.OBSERVE FREQUENCY= 300.0112289 ##.OBSERVE NUCLEUS= ^1H $$solvent=CDCl3 ##.FIELD= 7.05 $$ Tesla ##.ACQUISITION TIME= 3.7440000 $$ seconds ##.AVERAGES= 16 $$ number of transients ##RESOLUTION= 0.244 $$ digital resolution in Hz ##.SPINNING RATE= 20 $$ Hz ##.PHASE 0= -71.9 $$ zero order phase correction (left edge) ##.PHASE 1= 0.004827 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 499.955 $$ Referencing label $$ Varian specific parameters $$ -------------------------- ##$acqstatus= (0..1) 101 6 ##$alfa= 19.9999923706 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 3.744 ##$bs= 16 ##$celem= 1 ##$console= ##$cp= ##$ct= 16 ##$d1= 0 $$ sec ##$d2= 0 $$ sec ##$date= ##$dfrq= 300.0112289 $$ Hz ##$dm= ##$dmf= 200 ##$dmm= ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof= 0 $$ Hz ##$dp= ##$dpwr= 30 ##$dres= 1 ##$dseq= <> ##$exppath= ##$fb= 2000 ##$file= ##$filter= 54.0999984741 ##$fn1= 1024 ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$lb1= 0.318309992552 ##$lcpeak_= 0 ##$load= ##$lockfreq_= 46.0536521 $$ Hz ##$lockgain_= 48 ##$lockphase_= 97 ##$lockpower_= 44 ##$math= ##$method= ##$np= 29952 ##$nt= 16 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$parversion= 5.1 ##$pmode= ##$priority= 5 ##$probe_= <4nuc_30122> ##$proc1= ##$proc= ##$pslabel= ##$pw90= 19.9999866486 $$ usec ##$pw= 6.9999961853 $$ usec ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.9999961853 $$ usec ##$saveglobal_= (0..14) ##$seqfil= ##$sfrq= 300.0112289 ##$sn= 0 ##$solvent= ##$spin= 20 ##$ss= 0 ##$sw= 4000 ##$tin= ##$tn=

##$tof= 0 $$ Hz ##$tpwr= 55 ##$vloc_= ##$vproto_= <> ##$vrack_= 1 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$vzone_= 1 ##$wbs= <> ##$werr= <> ##$wexp= <> ##$wnt= <> ##$wshim= ##$wtfile1= <> ##$wtfile= <> ##$x1= 194 ##$x2y2= -62 ##$x3= -66 ##$x4= 0 ##$xy= 94 ##$xz2= 0 ##$xz= -117 ##$y1= 7 ##$y3= -76 ##$y4= 0 ##$yz2= 0 ##$yz= 272 ##$z0_= 845 ##$z1= -688 ##$z1c= -616 ##$z2= 1309 ##$z2c= -1504 ##$z2x2y2= 0 ##$z2x3= 0 ##$z2xy= 0 ##$z2y3= 0 ##$z3= 170 ##$z3c= 0 ##$z3x2y2= 0 ##$z3x3= 0 ##$z3x= 0 ##$z3xy= 0 ##$z3y3= 0 ##$z3y= 0 ##$z4= -82 ##$z4c= 0 ##$z4x2y2= 0 ##$z4x= 0 ##$z4xy= 0 ##$z4y= 0 ##$z5= 1 ##$z5x= 0 ##$z5y= 0 ##$z6= 0 ##$z7= 0 ##$z8= 0 ##$zx2y2= 0 ##$zx3= 0 ##$zxy= 0 ##$zy3= 0 ##$rp= -52.6 ##$lp= -19.3 ##$rfl= 500.0 ##$rfp= 0.0 ##$refpos= 0.0 ##$reffrq= 300.0 ##$axis=

##$sp= -500.0 ##$wp= 4000.0 ##$cr= 2899.7 ##$delta= 200.0 $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.244140625 ##XUNITS= HZ ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 0.244140625000 ##YFACTOR= 0.004944029 ##FIRSTX= 3999.755859375 ##LASTX= 0.000000000 ##MAXY= 162.001009 ##MINY= -0.192817 ##NPOINTS= 16384 ##FIRSTY= 0.000000 ##XYDATA= (X++(Y..Y)) 16383@Kk%j%J%jLjT%VKk%KmKjJ%TjLjT%VjJ%WjTKJkJ%TjLjT%TjJ%VjJ%Vj%JjLk%TJj%TKkjJ%V 16297@jJjKkJTjLl%WJj%jJT%j%TkK%Jj%UJjTLmK%TjJ%UkK%TjKj%jJjJ%TKmLj%TkK%Jj%jJ%TJ 16220A%kJ%UJ%j%VJ%kJT%j%TjJ%JjTJ%jJjJ%TKkJ%j%Jj%TJkJ%ZkKJ%kJKk%kLj%TjJ%TjJkKTl 16139aJ%WJjkJLlJTj%TjJ%JjkLj%WjJ%VKk%XjJjJ%UJjJj%jJ%WlL%TjJ%TKk%JkJj%Kj%Jj%WjK 16048AkKkKmNlKkJ%J%j%kKTkJmNkjJT%TkJ%TLl%WjJTjKk%JmL%J%kJ%TJjT%Kj%j%J%UjJ%s%jJ 15965@%JjKjTJk%KjTKj%Tj%J%TJjTJ%Jj%jJjJ%JkJ%WjJjLk%UJk%Kj%jKjJjTJ%JjTkMjJj%VjJ 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666@JkJjJjJ%TJj%Vj%KJk%VjJj%KjTLk%TJjTJkLj%TJj%UjJ%sLlKmK%TJTk%JjKmK%TkMk%jJjJ 580@%jKj%kKjJjJTkKkJjKj%VjJKkTK%UJTlKj%TKkjJ%UjKj%jJ%UJkJKkJ%kJ%jJ%jKjJj%Jj%jJ 501@%UJkJ%WJkJjJ%VjJTjJj%TKk%TjJKkj%J%Jj%UJj%JjJjkK%Jj%j%TJ%TJmL%UjJ%jJ%jJjKk% 419aJ%JkJjJjKJk%XJj%jTKTk%UKlJjKj%JjTJjJ%VJTk%TjJ%UJj%TJj%TjLk%kL%lL%j%jJ%YkLj 332@%VKlJ%TJkJ%UJjTKjKlJ%VJkJ%UjJ%WkKJk%JTkJKk%TJ%j%VJkJ%KkJj%jKjTJjJ%TKmK%YkK 242@JjJjTJTj%UjJKk%jJ%jJ%TJjJj%kLlJUkKj%Tj%JKmK%TJj%TKkKk%TjJ%ZjJ%TJkJ%VJ%Tj%T 158@jJkLj%UJj%TjJKk%VKk%TkLj%j%KJkjJ%jJTlJTKj%kJ%TJj%UjKjJ%jTJjLjTKmKkKLljJ%Tj 80aLlJjNm%lL%VKkjJ%TJ%kKj%kK%UJj%jJkMk%UKk%VKkKkJjkK%jJTkJjJ%UjKk%jJKj%kKjKj 0@ $$ checkpoint ##END= ##TITLE= STANDARD PROTON PARAMETERS ##JCAMP-DX= 5.00 $$ Varian, Inc., VNMR Software $$ VNMR Version 6.1 Revision C, March 8, 2004 $$ Sat Dec 23 18:01:37 EST 2006 $$ svsj version 6.1, 2000-01-29 ##DATA TYPE= NMR SPECTRUM ##DATA CLASS= XYDATA ##ORIGIN= ana ##OWNER= bradley ##SPECTROMETER/DATA SYSTEM= Varian UNITY INOVA-500 ##.OBSERVE FREQUENCY= 499.4774553 $$ MHz ##.OBSERVE NUCLEUS= ^1H $$solvent=CDCl3 ##.FIELD= 11.73 $$ Tesla ##.ACQUISITION TIME= 1.8920000 $$ seconds ##.AVERAGES= 8 $$ number of transients ##RESOLUTION= 0.488 $$ digital resolution in Hz ##.SPINNING RATE= 20.0 $$ Hz ##.PHASE 0= 36.1 $$ zero order phase correction (left edge) ##.PHASE 1= 0.001012 $$ first order phase correction, deg/Hz ##$REFERENCE_POINT= 1473.055 $$ Referencing label $$ distance of the zero axis position (in Hz) from the last data $$ point (right edge); positive values -> right edge is below 0 Hz $$ $$ Varian specific parameters $$ -------------------------- ##$acqcycles= 1 ##$acqdim= 1 ##$acqstatus= (0..1) 101 18 ##$alfa= 0 $$ usec ##$alock= ##$array= <> ##$arraydim= 1 ##$arrayelemts= 0 ##$at= 1.892 ##$bs= 32 ##$celem= 1 ##$console= ##$cp= ##$ct= 8 ##$d1= 0 $$ sec ##$d2= 0 $$ sec ##$dataProcessed= 0 ##$dataid= <> ##$date= ##$datname= <> ##$dfrq2= 0 ##$dfrq= 499.4774553 $$ Hz ##$dm2= ##$dm= ##$dmf2= 200 ##$dmf= 200 ##$dmm2= ##$dmm= ##$dn2= <> ##$dn=

##$dod= 0.00999999977648 $$ sec ##$dof2= 0 $$ Hz ##$dof= 0 $$ Hz ##$dp= ##$dpwr2= 1 ##$dpwr= 30 ##$dres2= 1 ##$dres= 1 ##$dseq2= <> ##$dseq= <> ##$exppath= ##$fb= 4000 ##$fidid= <> ##$file= ##$filter= 54.0999984741 ##$gain= 10 ##$homo2= ##$homo= ##$hs= ##$hst= 0.00800000037998 $$ sec ##$il= ##$in= ##$investigator= <> ##$lcpeak_= 0 ##$load= ##$lockfreq_= 76.673 $$ Hz ##$lockgain_= 48 ##$lockphase_= 37 ##$lockpower_= 20 ##$method= ##$notebook= <> ##$np= 30272 ##$nt= 8 ##$p1= 0 $$ usec ##$pad= 0.5 $$ sec ##$page= <> ##$paramChanged= 0 ##$parversion= 5.1 ##$pmode= ##$priority= 5 ##$probe_= ##$proc= ##$procdim= 1 ##$processid= 0 ##$pslabel= ##$pw90= 8.8 $$ usec ##$pw= 5.5499958992 $$ usec ##$ref= 0 $$ Hz ##$rfband= ##$rof1= 10 $$ usec ##$rof2= 9.99999904633 $$ usec ##$samplename= <> ##$saveglobal_= (0..14) ##$seqfil= ##$sfrq= 499.4774553 ##$shims= <> ##$sn= 0 ##$solvent= ##$spin= 20 ##$ss= 0 ##$sw= 8000 ##$temp= 25 ##$time_plotted= <> ##$time_processed= <20061223T180116> ##$time_run= <20061223T180035> ##$time_submitted= <20061223T180035> ##$time_submitted_local= <20061223T180035X06PMSatDec> ##$time_svfdate= <20061223T180035> ##$tin= ##$tn=

##$tof= 0 $$ Hz ##$tpwr= 55 ##$username= ##$vloc_= ##$vproto_= <> ##$vrack_= 1 ##$vtc= 25 ##$vtwait= 300 $$ sec ##$vzone_= 1 ##$wbs= <> ##$wdone= ##$werr= <> ##$wexp= ##$wnt= ##$wshim= ##$wtfile= <> ##$x1= 2897 ##$x2y2= 3716 ##$x3= -1585 ##$x4= -2900 ##$xy= -8640 ##$xz2= 13687 ##$xz= -279 ##$y1= -385 ##$y3= -7531 ##$y4= -10845 ##$yz2= 4898 ##$yz= 1427 ##$z0_= 8982 ##$z1= -2695 ##$z1c= -1044 ##$z2= -1406 ##$z2c= 196 ##$z2x2y2= -2816 ##$z2x3= -8577 ##$z2xy= 1376 ##$z2y3= 16775 ##$z3= 1478 ##$z3c= 0 ##$z3x2y2= 2793 ##$z3x3= 659 ##$z3x= -1782 ##$z3xy= -1511 ##$z3y3= -2802 ##$z3y= -5671 ##$z4= -23 ##$z4c= 0 ##$z4x2y2= 898 ##$z4x= 8409 ##$z4xy= -5169 ##$z4y= -882 ##$z5= 8803 ##$z5x= -2266 ##$z5y= -6499 ##$z6= -11755 ##$z7= -1776 ##$z8= 0 ##$zx2y2= 2985 ##$zx3= 486 ##$zxy= -3461 ##$zy3= -2828 ##$rfl= 1473.1 $$ Hz ##$rfp= 0.0 $$ Hz ##$reffrq= 499.4749284 $$ MHz ##$axis=

##$dmg= ##$rp= 44.2 ##$lp= -8.1 ##$sp= -1472.7 $$ Hz ##$wp= 7999.5 $$ Hz ##$cr= 0.0 $$ Hz ##$delta= 400.0 $$ Hz $$ $$ End of Varian specific parameters $$ --------------------------------- $$ Y-values stored with standard (16-bit) integer precision ##DELTAX= -0.488281250 ##XUNITS= HZ ##YUNITS= ARBITRARY UNITS $$ (mm on paper) ##XFACTOR= 0.488281250000 ##YFACTOR= 0.004944065 ##FIRSTX= 7999.511718750 ##LASTX= 0.000000000 ##MAXY= 162.002177 ##MINY= -0.069217 ##NPOINTS= 16384 ##FIRSTY= 0.000000 ##XYDATA= (X++(Y..Y)) 16383@%jJ%VkjLm%KjLkJ%jTOojJMj%TJTk%JTk%Llj%TJjLkKTmKkLlJ%JmK%TMnLlJkK%kNlLnLj 16309@%LlMjJkKkT%jMkl%JjJ%kLk%JTjK%jJjTKj%JKj%jkMm%LnJKkKjmKkLJTKpMJj%JTjK%kK% 16237BjTkNn%K%XjKJk%K%JjqO%TkKlL%kLlK%Vj%JTj%TMnL%TjTLnK%s%TkjPmj%KnK%KLlLjTkN 16152DmKkJ%TjTMoKmMjMl%LkJlj%kLjLjKJk%UkK%kKJMKrNpNjJKkj%TJ%kJ%TJj%UkK%UJj%JjJ 16077A%JjJ%kTKjKmKMpNjTJ%jTKjJoKkNkJTjPlmKlMJk%WkTKT%JMnJjnN%JKmKmLlL%Jj%JkLk% 16002@jLjTJjkMlKkKjJT%JKlLnKkjJkjOjJljKkJjkNJKk%mlJLjJKUjkl%kjTJKLmKlj%KT%LjkK 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